Sodium methanesulfinate → HCID 69635712, compound

Participants

Reaction Steps

4-(3-Methanesulfonylmethylphenyl)piperazine-1-carboxylic acid tert-butyl ester may be prepared in the following manner: on carrying out the operation according to the procedure of Example 10 starting with 1.55 g of 4-(3-chloromethylphenyl)piperazine-1-carboxylic acid tert-butyl ester and 0.766 g of sodium methanesulfinate, 0.9 g of 4-(3-methanesulfonyl-methylphenyl)piperazine-1-carboxylic acid tert-butyl ester is obtained in the form of a beige powder.

Provenance & Evidence