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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1058933Generated: November 2, 2026

Dimethylformamide dimethyl acetal → HCID 69686497, compound

https://huagongshe.com/reaction/1058933

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamide dimethyl acetalHCID 78373—
ReactantHCID 18669456HCID 18669456—
ProductHCID 69686497HCID 69686497—

Reaction Conditions

Temperature100 °C

Reaction Steps

A mixture of 13.4 g of 3-isopropyl-1-methyl-imidazolidine-2,4-dione and 13.6 ml dimethylformamide dimethylacetal were heated at 100° C. over the weekend. The reaction mixture was cooled to rt and purified by flash chromatography to give 9.9 g of a golden oil. Mass spectrum (EI) m/z 211 M+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06518293B2
Source datasetuspto-grants-2003_02
ORD IDord-2fbc136e225a4768a03f048ba60ae049
Source noteuspto-grants-2003_02