Dimethylformamide dimethyl acetal → HCID 69686497, compound

HRID 1058933Notes

Reaction equation

HRID 1058933 reaction equation
[CH:1]([N:4]1[C:8](=[O:9])[CH2:7][N:6]([CH3:10])[C:5]1=[O:11])([CH3:3])[CH3:2].CO[CH:14](OC)[N:15]([CH3:17])[CH3:16]>>[CH3:14][N:15]([CH:17]=[C:7]1[N:6]([CH3:10])[C:5](=[O:11])[N:4]([CH:1]([CH3:3])[CH3:2])[C:8]1=[O:9])[CH3:16]

Participants

3

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 18669456HCID 18669456, compound

Product 1

HCID 69686497HCID 69686497, compound

Conditions

Temperature
100 °C

Procedure

A mixture of 13.4 g of 3-isopropyl-1-methyl-imidazolidine-2,4-dione and 13.6 ml dimethylformamide dimethylacetal were heated at 100° C. over the weekend. The reaction mixture was cooled to rt and purified by flash chromatography to give 9.9 g of a golden oil. Mass spectrum (EI) m/z 211 M+.

Workup

  1. temperatureThe reaction mixture was cooled to rt
  2. custompurified by flash chromatography

Sources & evidence

ORD record
ord-2fbc136e225a4768a03f048ba60ae049
Source dataset
uspto-grants-2003_02
Patent number
US06518293B2

Reaction notes

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