HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18669451, compound → 2,4-Imidazolidinedione, 1-methyl-3-(1-methylethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18669451 | HCID 18669451 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,4-Imidazolidinedione, 1-methyl-3-(1-methylethyl)- | HCID 18669456 | 100.3% |
Reaction Steps
A mixture of 14.9 g of (3-isopropyl-1-methylureido)acetic acid in 50 ml of water and 50 ml of concentrated hydrochloric acid was refluxed for 2 h. On cooling the mixture was diluted with water and extracted with ethyl acetate to give 13.4 g of a colourless oil. Mass spectrum (EI) m/z 156 M+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518293B2 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-cca452dc76f3472080a859b30d98b049 |
| Source note | uspto-grants-2003_02 |