Stannous chloride dihydrate → HCID 178418788, compound

HRID 10590Notes

Reaction equation

HRID 10590 reaction equation
O.O.[Sn](Cl)Cl.[OH:6][C:7]1[C:16]2[C:11](=[C:12]([N+:17]([O-])=O)[CH:13]=[CH:14][CH:15]=2)[C:10]([Br:20])=[CH:9][N:8]=1>>[OH:6][C:7]1[C:16]2[C:11](=[C:12]([NH2:17])[CH:13]=[CH:14][CH:15]=2)[C:10]([Br:20])=[CH:9][N:8]=1

Participants

3

Procedure

According to the method of Example 114, Step A, a reduction reaction with tin(II) chloride dihydrate was performed by using Intermediate 137 to obtain the title compound.

Sources & evidence

ORD record
ord-68a2a3cab0e14ea68b8e17f3298801c9
Source dataset
uspto-grants-2006_08
Patent number
US07094789B2

Reaction notes

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