HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → N-benzyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | N-allyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine | HCID 11207972 | — |
| Reactant | Tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine | HCID 22182216 | — |
| Product | N-benzyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine | HCID 22598530 | 92% |
Reaction Steps
The compound is prepared in analogy to compound (204) from tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine and benzylbromide in 92% yield as colorless oil. Elemental analysis calculated for C19H32N2O2: C 71.21%; H 10.06%; N 8.74%. Found: C 71.22%; H 10.07%; N 8.94%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518326B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-1961c034242847b5ab512583739454df |
| Source note | uspto-grants-2003_02 |