Azobisisobutyronitrile → HCID 23563830, compound

HRID 1059041Notes

Reaction equation

HRID 1059041 reaction equation
[C:1]([C:3]([O:6][N:7]([C:15]([CH3:18])([CH3:17])[CH3:16])[C:8]([CH3:14])([CH3:13])[C:9]([NH:11][CH3:12])=[O:10])([CH3:5])[CH3:4])#[N:2].N(C(C)(C)C#N)=N[C:21](C)([CH3:24])[C:22]#N>>[C:1]([C:3]([O:6][N:7]([C:15]([CH3:18])([CH3:17])[CH3:16])[C:8]([CH3:14])([CH3:13])[C:9]([NH:11][CH2:12][CH2:22][CH2:21][CH3:24])=[O:10])([CH3:5])[CH3:4])#[N:2]

Participants

3

Reactant 2

HCID 6547AzobisisobutyronitrileHCID 22598524HCID 22598524, compound

Product 1

HCID 23563830HCID 23563830, compoundYield 48%

Procedure

The compound is prepared in analogy to compound (201) from the nitroxide (103) and azobisisobutyronitrile in 48% yield as colorless oil.

Sources & evidence

ORD record
ord-912b41e50f874fcca86711242ed8315a
Source dataset
uspto-grants-2003_02
Patent number
US06518326B1

Reaction notes

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