HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-amino-N-cyclohexylacetamide → HCID 178514400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-amino-N-cyclohexylacetamide | HCID 408592 | — |
| Reactant | 1-Aminoiminomehtylpyrazole hydrochloride | HCID 69066159 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178514400 | HCID 178514400 | 84% |
Reaction Steps
A round-bottomed flask is charged with 15 g of 2-amino-N-(cyclohexyl)-acetamide, 14,6 g 1-aminoiminomehtylpyrazole hydrochloride and 100 ml of dioxane. After 18 h stirring at reflux, the reaction medium is cooled to room temperature and precipitate which has formed is filtered off with suction. 16 g of a white solid are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518458B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-c752f4e9d50c47168940e60c8974c0b0 |
| Source note | uspto-grants-2003_02 |