HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 178466228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 1-(4'-fluoro[1,1'-biphenyl]-3-yl)-1-(1-trityl-1H-imidazol-4-yl)-1-ethanol | HCID 18668514 | — |
| Product | HCID 178466228 | HCID 178466228 | 68.8% |
Reaction Steps
By the reaction in the same manner as in Example 4-(iii) using 1-(4′-fluoro[1,1′-biphenyl]-3-yl)-1-(1-trityl-1H-imidazol-4-yl)-1-ethanol (1.51 g) and pyridine hydrochloride (599 mg), the title compound (559 mg) was obtained as colorless plate crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518257B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-5c0221903f5b4fa6bb8a811e176e7ff7 |
| Source note | uspto-grants-2003_02 |