HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → N-(3-Bromo-4-fluorophenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-Bromo-1-fluoro-4-nitrobenzene | HCID 69699 | — |
| Catalyst | Iron | HCID 23925 | — |
| Product | N-(3-Bromo-4-fluorophenyl)acetamide | HCID 18668623 | — |
Reaction Steps
By the reaction in the same manner as in Example 33-(i) using 2-bromo-1-fluoro-4-nitrobenzene (2.27 g), iron powder (2.90 g) and acetic anhydride (2.0 ml), the title compound (2.28 g) was obtained as colorless powder crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518257B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-057f7f76f0ed40d791171240f6b53df6 |
| Source note | uspto-grants-2003_02 |