HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 178450098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | N-cyclopropyl-4'-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl][1,1'-biphenyl]-3-carboxamide | HCID 18668572 | — |
| Product | HCID 178450098 | HCID 178450098 | 29% |
Reaction Steps
By the reaction in the same manner as in Example 4-(iii) using N-cyclopropyl-4′-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl][1,1′-biphenyl]-3-carboxamide (2.13 g) and pyridine hydrochloride (650 mg), the title compound (375 mg) was obtained as colorless powder crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518257B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-63961c582c084933b7e9ba461d5c02c3 |
| Source note | uspto-grants-2003_02 |