HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 178485488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 2-{4-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl]phenyl}-N-methylisonicotinamide | HCID 18668636 | — |
| Product | HCID 178485488 | HCID 178485488 | 41.3% |
Reaction Steps
By the reaction in the same manner as in Example 4-(iii) using 2-{4-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl]phenyl}-N-methylisonicotinamide (0.450 g) and pyridine hydrochloride (230 mg), the title compound (110 mg) was obtained as a colorless amorphous powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518257B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-b77654e5bee5432b96d896f39b2a2788 |
| Source note | uspto-grants-2003_02 |