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HRID1059723

反应详情

EQUATION

反应方程式

HRID 1059723 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)Cl
HCID31297

Methanesulfonyl chloride

CH3ClO2S

结构：CC(C)(C)OC(=O)N1Cc2ccc(O)cc2C1
HCID18630963

tert-Butyl 5-hydroxy-1,3-dihydro-2H-isoindole-2-carboxylate

C13H17NO3

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1Cc2ccc(OS(C)(=O)=O)cc2C1
HCID18630965

1,1-Dimethylethyl 1,3-dihydro-5-[(methylsulfonyl)oxy]-2H-isoindole-2-carboxylate

C14H19NO5S

收率 69%

PROCEDURE

实验过程

The title compound (2.3 g, 69%) was prepared from 2-(tert-butyloxycarbonyl)-5-hydroxy-2,3-dihydro-1H-isoindole (2.5 g) and methanesulfonyl chloride (1.7 ml) using the method of Description 6.