HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 10216479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 22344723 | HCID 22344723 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10216479 | HCID 10216479 | — |
Reaction Steps
A solution of Example 51A in methanol:THF (1 mL:1 mL) was treated with 10% palladium on carbon (30 mg), stirred under with hydrogen (1 atm) for 2 hours, filtered through diatomaceous earth (Celite®), and concentrated to provide the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521658B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-fcafb012ce484379a6fc066689d3ece9 |
| Source note | uspto-grants-2003_02 |