HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54513511, compound → 4-Isopropyloxy-2-methylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54513511 | HCID 54513511 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 4-Isopropyloxy-2-methylpyridine | HCID 18667573 | 78.7% |
Reaction Steps
A suspension of 4-isopropyloxy-2-methylpyridine N-oxide (0.78 g) in 2-propanol (10 ml) was hydrogenated over Raney-nickel (50% suspension in water, 1 ml) under a hydrogen atmosphere for 48 hours. The catalyst was filtered off, and the filtrate was evaporated under reduced pressure to give 4-isopropyloxy-2-methylpyridine (555 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521643B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-5308d304416e473dab3b9bf7ec755edf |
| Source note | uspto-grants-2003_02 |