HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18631011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 18667517 | HCID 18667517 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18631011 | HCID 18631011 | — |
Reaction Steps
To a solution of methylamine in tetrahydrofuran (2M, 11 ml) was added 1-fluoro-4-(4-methoxypyridin-2-yl)-2-nitrobenzene (289 mg). The mixture was stirred at ambient temperature for 2 hours and poured into water. The precipitate was collected by filtration and dried to give 1-methylamino-4-(4-methoxypyridin-2-yl)-2-nitrobenzene (280 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521643B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-a2c13635851f48c99bef068d32f0a0d0 |
| Source note | uspto-grants-2003_02 |