HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18667621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | HCID 18667517 | HCID 18667517 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18667621 | HCID 18667621 | — |
Reaction Steps
To a solution of ethylamine in ethanol (20% w/w, 2 ml) was added 1-fluoro-4-(4-methoxypyridin-2-yl)-2-nitrobenzene (200 mg). The mixture was stirred at ambient temperature for 4 hours and poured into water. The precipitate was collected by filtration and dried to give 1-ethylamino-4-(4-methoxypyridin-2-yl)-2-nitrobenzene (206 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521643B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-356955781f86442a8db51ade840c7085 |
| Source note | uspto-grants-2003_02 |