化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → N-[(5-Isoquinolyl)sulfonyl]-1,4-xylylenediamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | N-(tert-butoxycarbonyl)-N'-[(5-isoquinolyl)sulfonyl]-1,4-xylylenediamine | HCID 69523966 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | N-[(5-Isoquinolyl)sulfonyl]-1,4-xylylenediamine | HCID 69524387 | 80.5% |
反応手順
According to Reference Example 5, Step C, a reaction was performed by using Intermediate 60 (6 g) and 10% hydrogen chloride in methanol (20 ml) to obtain the title compound (3.7 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07094789B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-91463f1115d148529346c0f15f210d9b |
| 出典メモ | uspto-grants-2006_08 |