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HRID10602

反应详情

EQUATION

反应方程式

HRID 10602 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NCc1cccc(CN)c1
HCID2756043

tert-Butyl {[3-(aminomethyl)phenyl]methyl}carbamate

C13H20N2O2

结构：Cl.O=S(=O)(Cl)c1cccc2cnccc12
HCID13116932

Isoquinoline-5-sulfonyl chloride--hydrogen chloride (1/1)

C9H7Cl2NO2S

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCc1cccc(CNS(=O)(=O)c2cccc3cnccc23)c1
HCID69525002

未命名化合物

收率 78.1%

PROCEDURE

实验过程

According to Reference Example 5, Step B, a reaction was performed by using isoquinoline-5-sulfonyl chloride hydrochloride (9 g) and Intermediate 62 (8 g) to obtain the title compound (11.3 g).