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HRID1060348

反应详情

EQUATION

反应方程式

HRID 1060348 的结构方程式

REACTANTS

反应物

2
结构：Clc1ccc(OCC2CO2)cc1
HCID91515

2-[(4-Chlorophenoxy)methyl]oxirane

C9H9ClO2

结构：COc1ccc(CC(C)(C)N)cc1
HCID91892

2-(4-Methoxyphenyl)-1,1-dimethylethylamine

C11H17NO

PRODUCTS

生成物

1
结构：COc1ccc(CC(C)(C)NCC(O)COc2ccc(Cl)cc2)cc1.Cl
HCID18459608

未命名化合物

收率 135.9%

PROCEDURE

实验过程

Using the method of Example 6, supra, 4-chlorophenyl glycidyl ether (185 mg, 1 mmol) and 1,1-dimethyl-2-(4-methoxyphenyl)ethylamine (269 mg, 1.5 mmol) were used to prepare 272 mg of the title compound as a white solid: GC/EI-MS, m/z (rel. int.) 348 (M-15, 1), 244 (35), 243 (15), 242 (100), 163 (9), 121 (24), 114 (7), 71 (24), 70 (26), 58 (15), 42 (7).