Triethylene glycol monomethyl ether → HCID 18629479, compound

HRID 1060781Notes

Reaction equation

HRID 1060781 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][O:5][CH2:6][CH2:7][O:8][CH2:9]CO.ClC([O:15][CH:16]([Cl:18])[CH3:17])=O.ClC(OCCl)=[O:21]>>[C:9](=[O:21])([O:8][CH2:7][CH2:6][O:5][CH2:4][CH2:3][O:2][CH3:1])[O:15][CH:16]([Cl:18])[CH3:17]

Participants

4

Reactant 3

HCID 8178Triethylene glycol monomethyl etherHCID 62754Chloromethyl chloroformateHCID 5213051-Chloroethyl chloroformate

Product 1

HCID 18629479HCID 18629479, compound

Procedure

This compound was prepared by following the procedure described in Preparation 1 but substituting diethylene glycol monomethylether for triethyleneglycol monomethylether and 1-chloroethyl chloroformate for chloromethyl chloroformate. Colourless oil, b.p.: 82-88° C. at 0.03 mbar.

Workup

  1. customThis compound was prepared
  2. customdescribed in Preparation 1

Sources & evidence

ORD record
ord-1e6d1fe8a1884b98bd78ce0936f0beae
Source dataset
uspto-grants-2003_02
Patent number
US06525077B2

Reaction notes

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