HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloromethyl chlorosulfate → Chloromethyl 2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloromethyl chlorosulfate | HCID 2733556 | — |
| Reactant | 2,5,8,11-Tetraoxatridecan-13-oic acid | HCID 9859324 | — |
| Product | Chloromethyl 2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy-acetate | HCID 19611287 | — |
Reaction Steps
This compound was prepared from 2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy-acetic acid and chloromethyl chlorosulfate as described in the general procedure given in Synthetic Communications 14, 857-864 (1984). The resulting oil was purified by distillation in vacuo, b.p.: 130-132° C. at 0.06 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06525077B2 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-939498f9f5fa4f8088b5cdd56e903fa1 |
| Source note | uspto-grants-2003_02 |