Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1060889Generated: October 31, 2026

Hydrochloric Acid → HCID 86758854, compound

https://huagongshe.com/reaction/1060889

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
Reactant1,4-DioxaneHCID 31275—
ReactantHCID 18629424HCID 18629424—
SolventMethanolHCID 887—
ProductHCID 86758854HCID 86758854—

Reaction Steps

N-[1-(4-cyano-3-fluoro-phenyl)-1-(3-pyridyl)-ethyl]-2-methylpropanesulfinamide (0.080 g, 0.232 mmol) was dissolved in MeOH (5 mL) and treated with 4M HCl solution in dioxane (0.58 mL, 2.32 mmol). The solution was stirred for 4 h, concentrated to dryness, and azeotroped with CH2Cl2 and Et2O to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06525074B2
Source datasetuspto-grants-2003_02
ORD IDord-54252ce68eb24bacad2e62c126ef2ad8
Source noteuspto-grants-2003_02