N,N-Dimethylethylenediamine → HCID 69701207, compound

HRID 1061080Notes

Reaction equation

HRID 1061080 reaction equation
[C:1]([CH:4]1[CH2:9][N:8]([S:10]([C:13]2[CH:22]=[CH:21][C:20]3[C:15](=[CH:16][CH:17]=[C:18]([Cl:23])[CH:19]=3)[CH:14]=2)(=[O:12])=[O:11])[CH2:7][CH2:6][N:5]1[C:24]([C:26]1[CH:31]=[CH:30][C:29]([C:32]2[CH:37]=[CH:36][N+:35]([O-:38])=[CH:34][CH:33]=2)=[CH:28][CH:27]=1)=[O:25])([OH:3])=O.[CH3:39][N:40]([CH3:44])[CH2:41][CH2:42][NH2:43]>>[Cl:23][C:18]1[CH:19]=[C:20]2[C:15](=[CH:16][CH:17]=1)[CH:14]=[C:13]([S:10]([N:8]1[CH2:7][CH2:6][N:5]([C:24]([C:26]3[CH:27]=[CH:28][C:29]([C:32]4[CH:37]=[CH:36][N+:35]([O-:38])=[CH:34][CH:33]=4)=[CH:30][CH:31]=3)=[O:25])[CH:4]([C:1]([NH:43][CH2:42][CH2:41][N:40]([CH3:44])[CH3:39])=[O:3])[CH2:9]1)(=[O:12])=[O:11])[CH:22]=[CH:21]2

Participants

3

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 69700877HCID 69700877, compound

Product 1

HCID 69701207HCID 69701207, compound

Procedure

In a similar manner to Example 4 except for the use of 4-[4-[[2-carboxy-4-[(6-chloronaphthalen-2-yl)sulfonyl]piperazin-1-yl]carbonyl]phenyl]pyridine N-oxide and 2-(dimethylamino)ethylamine as the raw materials, the reaction was conducted, whereby the title compound was obtained.

Sources & evidence

ORD record
ord-c7e496310b054a0a94b6a8a64c163701
Source dataset
uspto-grants-2003_02
Patent number
US06525042B1

Reaction notes

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