HCID 22285712, compound → HCID 22285726, compound

Participants

Reaction Steps

A solution of the product from Step D (0.59 g, 2.6 mmol) in ethanol (20 mL) was treated as described in Step F of Example 1 to provide a solid (0.46 g, 54%): m.p 95-97° C.; MS (ES) m/z 323 (M+); 1H NMR (CDCl3) δ 7.34 (5H, m), 7.14 (1H, s), 5.08 (2H, s), 4.31 (2H, m), 4.13 (2H, m), 3.02 (5H, m), 2.19 (3H, m), 1.27(3H, t, J=6.0 Hz).

Provenance & Evidence