HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22285054, compound → HCID 22285066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22285054 | HCID 22285054 | — |
| Reactant | Monomethylamine methanol | HCID 57454252 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22285066 | HCID 22285066 | — |
Reaction Steps
7-Bromo-1-methoxynaphtho[1,2-c]furan-3(1H)-one (1.03 g) was dissolved in THF (10 mL), and 40% methylamine methanol solution (10 mL) was added. The reaction mixture was stirred at room temperature for 1 hr., and the solvent was evaporated to give the title compound (1.03 g) as pale-yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06960586B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-21300f5ad9274f81b97374f033624a5a |
| Source note | uspto-grants-2005_11 |