1,1-Dimethylhydrazine → HCID 178450033, compound

Participants

Reaction Steps

By a ring closure reaction, a detritylation reaction and purification in the same manner as in Example 1 using methyl 1-bromomethyl-6-[1-hydroxy-2-methyl-1-(1-H-imidazol-4-yl)propyl]-2-naphthoate (0.66 g) and 1,1-dimethylhydrazine (1.0 ml), the title compound (0.18 g) was obtained as a colorless amorphous solid.

Provenance & Evidence