Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2'-Chloro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester → Carbamic acid,(3-amino-2'-chloro[1,1'-biphenyl]-4-yl)-,1,1-dimethylethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2'-Chloro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester | HCID 69592813 | — |
| 촉매 | Nickel | HCID 935 | — |
| 생성물 | Carbamic acid,(3-amino-2'-chloro[1,1'-biphenyl]-4-yl)-,1,1-dimethylethyl ester | HCID 69592803 | — |
반응 단계
Prepared from (2′-chloro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example C8) by catalytic hydrogenation with Raney-Ni according to the general procedure G (method a). Obtained as a white solid (180 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06960578B2 |
| 출처 데이터셋 | uspto-grants-2005_11 |
| ORD ID | ord-f17211e8b781412385ba9f42ac019227 |
| 출처 메모 | uspto-grants-2005_11 |