Benzoic Acid → HCID 9914997, compound

HRID 1062332Notes

Reaction equation

HRID 1062332 reaction equation
[NH2:1][C@@H:2]([CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C@H:3]([OH:16])[CH2:4][N:5]([CH2:14][CH3:15])[NH:6][C:7]([O:9]C(C)(C)C)=O.C(O)(=O)[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1.[CH3:33][S:34]([NH:37][C:38]1[S:39][CH:40]=[C:41]([C:43](O)=[O:44])[N:42]=1)(=[O:36])=[O:35]>>[C:7]([NH:6][N:5]([CH2:4][C@@H:3]([OH:16])[C@@H:2]([NH:1][C:43]([C:41]1[N:42]=[C:38]([NH:37][S:34]([CH3:33])(=[O:36])=[O:35])[S:39][CH:40]=1)=[O:44])[CH2:17][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)[CH2:14][CH3:15])(=[O:9])[C:25]1[CH:26]=[CH:27][CH:28]=[CH:29][CH:30]=1

Participants

4

Reactant 3

HCID 243Benzoic AcidHCID 22051332HCID 22051332, compoundHCID 69611254HCID 69611254, compound

Product 1

HCID 9914997HCID 9914997, compound

Procedure

Synthesized as described above from tert-butyl 2-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-ethylhydrazinecarboxylate, benzoic acid and 2-methanesulfonylamino-thiazole-4-carboxylic acid. MS (ESI+) for C24H29N5O5S2 m/z 532.7 (M+H)+.

Workup

  1. customSynthesized

Sources & evidence

ORD record
ord-ed9fccdea0334d1294f6de5abb0fa19a
Source dataset
uspto-grants-2005_11
Patent number
US06960664B2

Reaction notes

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