Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 5-Chloro-N-(4-fluorophenyl)-2-nitroaniline | HCID 22282207 | — |
| Product | HCID 22282196 | HCID 22282196 | — |
Reaction Steps
36.44 g (5-chloro-2-nitrophenyl)-(4-fluorophenyl)amine was added to a solution that consists of 6.6 g of sodium in 450 ml of methanol, and it was refluxed for 16 hours. After another 30 hours of stirring at 60° C., it was cooled, and the crystalline product was suctioned off. 34 g of (5-methoxy-2-nitrophenyl)-(4-fluorophenyl)amine was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06962932B2 |
|---|
| Source dataset | uspto-grants-2005_11 |
|---|
| ORD ID | ord-b4e431d692464d37a9236750d5d5a837 |
|---|
| Source note | uspto-grants-2005_11 |
|---|
