HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 7-Chloro-N,N-dimethylthieno[3,2-b]pyridine-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Lithium 7-chlorothieno[3,2-b]pyridine-2-carboxylate | HCID 23677819 | — |
| Product | 7-Chloro-N,N-dimethylthieno[3,2-b]pyridine-2-carboxamide | HCID 22143537 | — |
Reaction Steps
The title compound was prepared from dimethyl amine and lithium 7-chloro-thieno[3,2-b]pyridine-2-carboxylate by a procedure analogous to Example 1B. MS: 239/241 (MH+); HPLC Rf: n.d.; HPLC purity: n.d.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06964961B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-495da16d536343cfb5a01b72782af5d0 |
| Source note | uspto-grants-2005_11 |