HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Amino-2-methylindole → 7-(2-Methyl-1h-indol-5-ylamino)-thieno[3,2-b]pyridine-2-carboxylic acid dimethylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Amino-2-methylindole | HCID 2733992 | — |
| Reactant | 7-Chloro-N,N-dimethylthieno[3,2-b]pyridine-2-carboxamide | HCID 22143537 | — |
| Product | 7-(2-Methyl-1h-indol-5-ylamino)-thieno[3,2-b]pyridine-2-carboxylic acid dimethylamide | HCID 69737370 | — |
Reaction Steps
The title compound was prepared from 2-methyl-1H-indol-5-ylamine and 7-chloro-thieno[3,2-b]pyridine-2-carboxylic acid dimethylamide by a procedure analogous to Example 1C. MS: 351 (MH+); HPLC Rf: 3.87 min.; HPLC purity: 94%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06964961B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-49fee27922634c6e93e6cc442a0ffd34 |
| Source note | uspto-grants-2005_11 |