N,N-Dimethylethylenediamine → HCID 91072374, compound

HRID 1063146Notes

Reaction equation

HRID 1063146 reaction equation
[CH3:1][N:2]([CH3:6])[CH2:3][CH2:4][NH2:5].[Cl:7][C:8]1[CH:13]=[CH:12][N:11]=[C:10]2[CH:14]=[C:15]([C:17]([O-])=[O:18])[S:16][C:9]=12.[Li+]>>[CH3:1][N:2]([CH3:6])[CH2:3][CH2:4][NH:5][C:17]([C:15]1[S:16][C:9]2[C:10](=[N:11][CH:12]=[CH:13][C:8]=2[Cl:7])[CH:14]=1)=[O:18]

Participants

3

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 23677819Lithium 7-chlorothieno[3,2-b]pyridine-2-carboxylate

Product 1

HCID 91072374HCID 91072374, compound

Procedure

The title compound was prepared from 2-dimethylaminoethyl amine and lithium 7-chloro-thieno[3,2-b]pyridine-2-carboxylate by a procedure analogous to Example 1B. MS: 284/286 (MH+); HPLC Rf: 3.47 min.; HPLC purity: 95%.

Sources & evidence

ORD record
ord-c3d2e111df854382a526d52b593acbb7
Source dataset
uspto-grants-2005_11
Patent number
US06964961B2

Reaction notes

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