2-Morpholinoethylamine → HCID 90906051, compound

HRID 1063158Notes

Reaction equation

HRID 1063158 reaction equation
[N:1]1([CH2:7][CH2:8][NH2:9])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[Cl:10][C:11]1[CH:16]=[CH:15][N:14]=[C:13]2[CH:17]=[C:18]([C:20]([O-])=[O:21])[S:19][C:12]=12.[Li+]>>[N:1]1([CH2:7][CH2:8][NH:9][C:20]([C:18]2[S:19][C:12]3[C:13](=[N:14][CH:15]=[CH:16][C:11]=3[Cl:10])[CH:17]=2)=[O:21])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 4082852-MorpholinoethylamineHCID 23677819Lithium 7-chlorothieno[3,2-b]pyridine-2-carboxylate

Product 1

HCID 90906051HCID 90906051, compound

Procedure

The title compound was prepared from 2-morpholine-4-yl-ethylamine and lithium 7-chloro-thieno[3,2-b]pyridine-2-carboxylate by a procedure analogous to Example 1B. MS: 326/328 (MH+); HPLC Rf: 3.45 min.; HPLC purity 94%.

Sources & evidence

ORD record
ord-16b3eac097e74b7c8f6d844c35a1e0b3
Source dataset
uspto-grants-2005_11
Patent number
US06964961B2

Reaction notes

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