HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethyl methyl ether → HCID 23401171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | 7-chloro-2-[(R)-3-hydroxypyrrolidine-1-carbonyl]thieno[3,2-b]pyridine | HCID 20767758 | — |
| Product | HCID 23401171 | HCID 23401171 | — |
Reaction Steps
The title compound was prepared from 1-bromo-2-methoxy-ethane and (3R)-(3-hydroxy-pyrrolidin-1-yl)-[7-chloro-thieno[3,2-b]pyridin-2-yl]-methanone by a procedure analogous to Example 67B. MS: 341.2/343.2 (MH+); HPLC Rf: 4.236 min.; HPLC purity: 77%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06964961B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-ea6b0d90527e4325a92a1d324ed53c55 |
| Source note | uspto-grants-2005_11 |