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HRID1063599

反应详情

EQUATION

反应方程式

HRID 1063599 的结构方程式

REACTANTS

反应物

3
结构：NO
HCID787

Hydroxylamine

H3NO

结构：CC(=O)[O-].[Na+]
HCID517045

Sodium Acetate

C2H3NaO2

结构：CCOP(=O)(OCC)c1ccc(C=O)o1
HCID46784019

未命名化合物

PRODUCTS

生成物

1
结构：CCOP(=O)(OCC)c1ccc(C=NO)o1
HCID86586426

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A solution of 5-diethylphosphono-2-furaldehyde (1 mmole) in ethanol was treated with hydroxylamine (1.1 mmole) and sodium acetate (2.2 mmole) at 25° C. for 12 h. Extraction and chromatography gave 5-diethylphosphono-2-furaldehyde oxime.

WORKUP

后处理

  1. extractionExtraction and chromatography