HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 23402343, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | N-benzyl-N-[(S)-valinyl]glycine Ethyl Ester | HCID 23402348 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23402343 | HCID 23402343 | 96% |
Reaction Steps
A solution of 4.2 gm (14.4 Mol) N-benzyl-N-[(S)-valinyl]glycine ethyl ester and 1.2 mL (0.98 mMol) pyridine in 85 mL toluene was heated at reflux for 3 hours. The reaction mixture was then concentrated under reduced pressure to provide 3.4 gm (96%) of the desired compound as an oily solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967201B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-9656edbda238490089920d8b71cb61c9 |
| Source note | uspto-grants-2005_11 |