HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bromide → Benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | HCID 23401651 | HCID 23401651 | — |
| Reactant | HCID 54024567 | HCID 54024567 | — |
| Product | Benzenesulfonamide | HCID 7370 | 6% |
Reaction Steps
4-chloro-N-2,5-dichlorophenyl)-N-3-(2-carboxymethyl-3-thiazolidinyl)-1(R)-methylpropyl)-benzenesulfonamide was prepared analogous to 4-chloro-N-(2,5-dichlorophenyl)-N-(3-(2-((methylsulfonyl)methyl)-1-piperidinyl)-1(R)-methylpropyl)benzenesulfonamide by reacting 4-chloro-N-[2,5-dichlorophenyl]-N-[(R)-1-methyl-3-bromopropyl]benzenesulfonamide with 2-carboxymethyl-3-thiazolidine. Yield=6%; White powder: IR (KBr) 1747, 1467, 1352, 1166, 1094, 622 cm−1; MS (ESI+), 537 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-63111a8559904ba1a0a067130cd39e53 |
| Source note | uspto-grants-2005_11 |