HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 23401698, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 23401648 | HCID 23401648 | — |
| Reactant | HCID 23401699 | HCID 23401699 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23401698 | HCID 23401698 | 67% |
Reaction Steps
4-chloro-N-(2,5-dichlorophenyl)-N-(5-(2-carboxy-3-thiazolidinyl)-1(R)-methylpentyl)benzenesulfonamide was prepared analogous to 4-chloro-N-(2,5-dichlorophenyl)-N-(3-(2-carboxy-3-thiazolidinyl)-1(R)-methylpropyl)benzenesulfonamide by reacting 4-chloro-N-(2,5-dichlorophenyl)-N-(5-(2-carboxymethyl-3-thiazolidinyl)-1(R)-methylpentyl)benzenesulfonamide with 50% aqueous KOH. Yield=67%; White foam: IR (neat, CH2Cl2) 1467, 1350, 1167, 1093, 753, 622 cm−1; MS (ESI+), 553 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-e1b9a1ada35c402b9d96e0ae472f7818 |
| Source note | uspto-grants-2005_11 |