Potassium Hydroxide → HCID 23401660, compound

Participants

Role	Name	HCID	Charge
Reactant	Potassium Hydroxide	HCID 14797	—
Reactant	Potassium Bromide	HCID 253877	—
Reactant	HCID 23401661	HCID 23401661	—
Reactant	HCID 86759907	HCID 86759907	—
Product	HCID 23401660	HCID 23401660	70%

Reaction Steps

4-chloro-N-(2,5-dichlorophenyl)-N-(3-(5-carboxy-3-thiazolidinyl)-1(R)-methylpropyl)benzenesulfonamide was prepared analogous to 4-chloro-N-2,5-dichlorophenyl)-N-(3-(2-carboxy-3-thiazolidinyl)-1(R)-methylpropyl)benzenesulfonamide by reacting 4-chloro-N-(2,5-dichlorophenyl)-N-(3-(5-carboxymethyl-3-thiazolidinyl)-1(R)-methylpropyl)benzenesulfonamide with 50% aqueous KOH. Yield=70%; White foam: IR (KBr) 1467, 1350, 1167, 1094, 753, 622 cm−1; MS (ESI+), 525 (M+H)+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06967196B1
Source dataset	uspto-grants-2005_11
ORD ID	ord-fbbd1274431f499a880d5d2b08fde359
Source note	uspto-grants-2005_11