HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 23401681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | HCID 23401648 | HCID 23401648 | — |
| Reactant | HCID 23401682 | HCID 23401682 | — |
| Product | HCID 23401681 | HCID 23401681 | 45% |
Reaction Steps
4-chloro-N-(2,5-dichlorophenyl)-N-(4-(5-carboxy-3-thiazolidinyl)-1(R)-methylbutyl)benzenesulfonamide was prepared analogous to 4-chloro-N-(2,5-dichlorophenyl)-N-(3-(2-carboxy-3-thiazolidinyl)-1(R)-methylpropyl)benzenesulfonamide by reacting 4-chloro-N-(2,5-dichlorophenyl)-N-(4-(5-carboxymethyl-3-thiazolidinyl)-1(R)-methylbutyl)benzenesulfonamide with 50% aqueous KOH. Yield=45%; White powder: IR (KBr) 1467, 1350, 1167, 1094, 754, 622 cm−1; MS (ESI+), 537 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-d003eeb4a4704597beb68dd4f7ec2e19 |
| Source note | uspto-grants-2005_11 |