HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonamide → HCID 86759908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 23401683 | HCID 23401683 | — |
| Product | HCID 86759908 | HCID 86759908 | 84% |
Reaction Steps
4-chloro-N-2,5-dichlorophenyl)-N-(4-[[(phenyl)carbonyl]amino]-1(R)-methylbutyl]benzenesulfonamide was prepared analogous to 4-chloro-N-[2,5-dichlorophenyl]-N-[(R)-1-methyl-4-(acetylamino)butyl]benzenesulfonamide by reacting 4-chloro-N-[2,5-dichlorophenyl]-N-[R]-1-methyl-4-aminobutyl]benzenesulfonamide with benzoyl chloride. Yield=84%; MS (ESI+), 525 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-6274eecdefeb44a8af8e62fb4d3ac8fa |
| Source note | uspto-grants-2005_11 |