HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 86759909, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | HCID 23401683 | HCID 23401683 | — |
| Product | HCID 86759909 | HCID 86759909 | 96% |
Reaction Steps
4-chloro-N-2,5-dichlorophenyl)-N-[4-[[(methoxy)carbonyl]amino]-1(R)-methylbutyl]benzenesulfonamide was prepared analogous to 4-chloro-N-[2,5-dichlorophenyl]-N-[(R)-1-methyl-4-(acetylamino)butyl]benzenesulfonamide by reacting 4-chloro-N-[2,5-dichlorophenyl]-N-[R]-1-methyl-4-aminobutyl]benzenesulfonamide with methyl chloroformate. Yield=96%; MS (ESI+), 479 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-365fda323d7f4b9e9ae0f2a8df9c328e |
| Source note | uspto-grants-2005_11 |