Hydrochloric Acid → HCID 136411685, compound

Participants

Reaction Steps

Preparation of the title compound from Intermediate 136(a) (0.16 g, 0.33 mmol) and 4M HCl in dioxane (1.6 mL, 6.6 mmol) was carried out analogously to Example 91. Isolation, also in an analogous manner, included a further trituration with CH2Cl2/diethyl ether and afforded the title compound (0.137 g) as an orange/yellow powder in 96% yield.

Provenance & Evidence