HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 135794602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 136181641 | HCID 136181641 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 135794602 | HCID 135794602 | — |
Reaction Steps
Preparation of the title compound from Intermediate 189(a) (136 mg, 0.291 mmol) and 4.0 M HCl in dioxane (1.5 mL) was carried out analogously to Example 91. Isolation, also in an analogous manner, afforded the title compound (75 mg, 0.186 mmol) as a yellow powder in 64% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967198B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-aae0af601b864c11accd9cfb3e33aeb1 |
| Source note | uspto-grants-2005_11 |