Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(3-Trifluoromethylsulfanylphenyl)oxoacetaldehyde → 3-(4-Methoxyphenyl)-5-(3-trifluoromethylsulfanylphenyl)-[1,2,4]triazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (3-Trifluoromethylsulfanylphenyl)oxoacetaldehyde | HCID 22273584 | — |
| 반응물 | HCID 178491255 | HCID 178491255 | — |
| 생성물 | 3-(4-Methoxyphenyl)-5-(3-trifluoromethylsulfanylphenyl)-[1,2,4]triazine | HCID 10067260 | — |
반응 단계
(3-Trifluoromethylsulfanylphenyl)oxoacetaldehyde was reacted with 4-methoxybenzenecarboximidic hydrazide hydriodide salt (1.11 g, 3.78 mmol) using the method described in Example 1 to give 3-(4-methoxyphenyl)-5-(3-trifluoromethylsulfanylphenyl)-[1,2,4]triazine as a yellow solid (820 g): δH (400 MHz, CDCl3) 3.92 (3H, s), 7.06-7.10 (2H, m), 7.67 (1H, t, J 7.8 Hz), 7.90 (1H, d, J 7.8 Hz), 8.35-8.39 (1H, m), 8.56 (1H, s), 8.60-8.64 (2H, m), 9.55 (1H, s); m/z (ES+) 364.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06969716B2 |
| 출처 데이터셋 | uspto-grants-2005_11 |
| ORD ID | ord-793728741e234943bcebd17f28f86f45 |
| 출처 메모 | uspto-grants-2005_11 |