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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1064564Generated: October 30, 2026

Hydrochloric Acid → HCID 131725227, compound

https://huagongshe.com/reaction/1064564

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantDiethyl EtherHCID 3283—
ReactantHCID 10158684HCID 10158684—
SolventDichloromethaneHCID 6344—
ProductHCID 131725227HCID 131725227—

Reaction Steps

The product from step (iii) (0.12 g) in dichloromethane was treated with 1M hydrogen chloride in diethyl ether (12 ml). The mixture was stirred at room temperature for 18 hours. The solvent was evaporated under reduced pressure to give the subtitle product as a pale yellow solid. Yield 0.15 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06969713B2
Source datasetuspto-grants-2005_11
ORD IDord-3f918e1f728e4fd28f73917c51967cb3
Source noteuspto-grants-2005_11