HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131725227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 10158684 | HCID 10158684 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131725227 | HCID 131725227 | — |
Reaction Steps
The product from step (iii) (0.12 g) in dichloromethane was treated with 1M hydrogen chloride in diethyl ether (12 ml). The mixture was stirred at room temperature for 18 hours. The solvent was evaporated under reduced pressure to give the subtitle product as a pale yellow solid. Yield 0.15 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06969713B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-3f918e1f728e4fd28f73917c51967cb3 |
| Source note | uspto-grants-2005_11 |