2-Methylpiperazine → HCID 22273359, compound

HRID 1064573Notes

Reaction equation

HRID 1064573 reaction equation
Cl[CH2:2][C:3]([NH:5][C:6]1[C:11]([CH3:12])=[CH:10][CH:9]=[CH:8][C:7]=1[CH3:13])=[O:4].[CH3:14][CH:15]1[CH2:20][NH:19][CH2:18][CH2:17][NH:16]1>>[CH3:13][C:7]1[CH:8]=[CH:9][CH:10]=[C:11]([CH3:12])[C:6]=1[NH:5][C:3](=[O:4])[CH2:2][N:19]1[CH2:18][CH2:17][NH:16][CH:15]([CH3:14])[CH2:20]1

Participants

3

Reactant 2

HCID 660572-MethylpiperazineHCID 707982-Chloro-N-(2,6-dimethylphenyl)acetamide

Product 1

HCID 22273359HCID 22273359, compound

Procedure

The subtitle compound was prepared from 2-chloro-N-(2,6-dimethylphenyl)acetamide (7 g) and (±)-2-methyl-piperazine (3.55 g) by the method of Example 15 step (ii) as a white solid. Yield 7 g.

Sources & evidence

ORD record
ord-7895c46eb5624023b155aa38bbd34bce
Source dataset
uspto-grants-2005_11
Patent number
US06969713B2

Reaction notes

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