Hydrochloric Acid → HCID 131725231, compound

HRID 1064576Notes

Reaction equation

HRID 1064576 reaction equation
[CH3:1][CH:2]1[N:7]([C:8]2[C:9]3[CH:16]=[CH:15][S:14][C:10]=3[N:11]=[CH:12][N:13]=2)[CH:6]([CH3:17])[CH2:5][N:4]([CH2:18][C:19]([NH:21][C:22]2[CH:27]=[C:26]([CH2:28][N:29]3[CH2:34][CH2:33][N:32](C(OC(C)(C)C)=O)[CH2:31][CH2:30]3)[CH:25]=[CH:24][C:23]=2[CH3:42])=[O:20])[CH2:3]1.[ClH:43]>O1CCOCC1>[ClH:43].[CH3:1][C@H:2]1[N:7]([C:8]2[C:9]3[CH:16]=[CH:15][S:14][C:10]=3[N:11]=[CH:12][N:13]=2)[C@@H:6]([CH3:17])[CH2:5][N:4]([CH2:18][C:19]([NH:21][C:22]2[CH:27]=[C:26]([CH2:28][N:29]3[CH2:30][CH2:31][NH:32][CH2:33][CH2:34]3)[CH:25]=[CH:24][C:23]=2[CH3:42])=[O:20])[CH2:3]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 131725230HCID 131725230, compound

Product 1

HCID 131725231HCID 131725231, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

The product from step (iii) (0.17 mg) was dissolved in 4M hydrogen chloride in 1,4-dioxane (2 ml). After 48 h the solvents were evaporated under reduced pressure to leave the title compound as a white solid. Yield: 0.16 g

Workup

  1. customAfter 48 h the solvents were evaporated under reduced pressure

Sources & evidence

ORD record
ord-16678d4ed20443028bd702138b71f052
Source dataset
uspto-grants-2005_11
Patent number
US06969713B2

Reaction notes

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