HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyanobenzene-1-sulfonyl chloride → Cis-2-(4-(3-Cyanobenzenesulphonyl)-3,5-dimethylpiperazin-1-yl)-N-(3-fluoro-2-methylphenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyanobenzene-1-sulfonyl chloride | HCID 2801360 | — |
| Reactant | cis-(3,5-Dimethylpiperazin-1-yl)-N-(2-methyl-3-fluorophenyl)acetamide | HCID 69746587 | — |
| Product | Cis-2-(4-(3-Cyanobenzenesulphonyl)-3,5-dimethylpiperazin-1-yl)-N-(3-fluoro-2-methylphenyl)acetamide | HCID 69745121 | — |
Reaction Steps
The title compound was prepared from the product of step (i) (0.503 mmol) and 3-cyanobenzenesulphonyl chloride (0.503 mmol) by the method of Example 58 step (ii) as a white solid. Yield: 44 mg
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06969713B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-805793a2c93c4281b13eddb30fa6336f |
| Source note | uspto-grants-2005_11 |